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Chemical Analysis of Contaminated Land

By K. Clive Thompson, Paul Nathanail

Published June 27th 2003 by Blackwell – 290 pages

Series: Sheffield Analytical Chemistry

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Description

With the wide range of techniques and options available for chemical analysis, and the great potential for today's methods to be superceded by tomorrow's technology, a how-to book on chemical analysis would be impractical, unnecessary, and quickly out of date. Yet professionals in the field need a resource detailing the strengths and limitations of such analyses if they are to use analytical results in an intelligent and informed manner.

Chemical Analysis of Contaminated Land explores how to choose the appropriate analyses, provides relevant strategies for carrying out analyses, and discusses methods of interpreting results within the new risk-based legislative framework for contaminated land. The book addresses all aspects of analysis, from delivery of samples to the laboratory to the presentation of results to clients. The editors provide concentrated, tabular data, highlight problems of analysis, and propose solutions. Special features include in-depth coverage of asbestos and techniques of ecotoxicity measurement.

Designed for use by chemists, scientists, or engineers responsible for analyzing potentially contaminated soil or water samples, Chemical Analysis of Contaminated Land is written in a style that helps both new and experienced practitioners. This book distills the expertise and experience of the authors to provide a one-stop resource on the chemical analysis of contaminated land.

Contents

THE RISK ASSESSOR AS THE CUSTOMER, K.C. Thompson and C.P. Nathanail

Analysis Issues

Definition Analysis

Quality Issues in Contaminated Land Analysis

Sampling Point Frequency Considerations

Sample Pre-Treatment Issues

Analysis Method Requirements

Measurement Uncertainty

Proficiency Schemes

New Areas of Analysis

THE REQUIREMENTS OF THE ANALYTICAL METHOD, D. Westwood

Need for Fully Documented and Properly Validated Methods

Current Regimes

How to Validate International, National, and Individual Laboratory Methods

Quality Control - Quality Assurance

Prescribed Method Versus Minimum Performance Characteristics Approach

Proficiency Testing for Contaminated Soil Analysis

Reference Materials

INITIAL SAMPLE PREPARATION, M. Allen

Introduction

An Overview of Initial Sample Preparation

Processes and Problems

Quality Control

Good Laboratory Practice in Initial Sample Preparation

References

METAL ANALYSIS, P. Thomas

Introduction

General Discussion

Overview of Instrumental Methods of Analysis

What is Atomic Emission Spectrometry?

How to Select the Proper Technique?

Overview of Trace Element Separation

References

ANALYSIS OF INORGANIC PARAMETERS, G.E. Rayment, R. Sadler, A. Craig, B. Noller, and B. Chiswell

Introduction

Electrical Conductivity

pH

Redox Potential

Water Soluble Chloride

Water Soluble Boron

Sulfur

Cyanides, Thiocyanates, and Cyanates

Asbestos

Abbreviations

Notes

References

PETROLEUM HYDROCARBONS AND POLYAROMATIC HYDROCARBONS, J. Farrell-Jones

Introduction

Environmental Fate of Petroleum Products

Factors Influencing the Analytical Process

Total Petroleum Hydrocarbons: A Detailed Method Review

Petroleum Group Type Analysis (Detailed Review)

Individual Compound Analysis

Polyaromatic Hydrocarbons (PAHs)

Abbreviations

Glossary of Terms

Bibliography

Editor's Note

VOLATILE ORGANIC COMPOUNDS, S. Owen and P. Whittle

Introduction

Presence of VOCs in Soil

Sampling and Sub-Sampling

Methods of Analysis

Chromatography

Detectors and Quantitation

Screening Techniques

Specific Groupings

References

Commonly Used Groupings for Analysing VOC Samples

NON-HALOGENATED ORGANIC COMPOUNDS INCLUDING SEMI-VOLATILE ORGANIC COMPOUNDS (SVOCS), J. Harmsen and P. Frintrop

Introduction

Extraction

Screening or Quantitative Determination

The Bioavailable Fraction

Detection, Identification, and Quantification

Examples

References

LEACHING TESTS, L. Heasman

Introduction

The Value of Leaching Tests in Land Contamination

The Primary Factors Which Control Leaching

Available Leaching Tests

Quality Assurance and Quality Control

Selection of a Leaching Test

Interpretation of the Results of Leaching Tests

References

ECOLOGICAL ASSESSMENT AND TOXICITY SCREENING IN CONTAMINATED LAND ANALYSIS, A.P. Loibner, O.H.J. Szolar, R. Braun, and D. Hirman

Introduction

Toxicity Testing

The Use of Bioassays for Soil Evaluation

Conclusion

Acknowledgements

Bioassays

Abbreviations

Refefences

Appendices

Name: Chemical Analysis of Contaminated Land (Hardback)Blackwell 
Description: By K. Clive Thompson, Paul Nathanail. With the wide range of techniques and options available for chemical analysis, and the great potential for today's methods to be superceded by tomorrow's technology, a how-to book on chemical analysis would be impractical, unnecessary,...
Categories: Analytical Chemistry, Environmental Sciences